Por favor, use este identificador para citar o enlazar a este item:
http://hdl.handle.net/10261/191946
COMPARTIR / EXPORTAR:
SHARE CORE BASE | |
Visualizar otros formatos: MARC | Dublin Core | RDF | ORE | MODS | METS | DIDL | DATACITE | |
Título: | Separation of disaccharides by comprehensive two-dimensional gas chromatography−time-of-flight mass spectrometry. Application to honey analysis |
Autor: | Brokl, M. CSIC; Soria, Ana C. CSIC ORCID ; Ruiz-Matute, Ana I. CSIC ORCID ; Sanz, M. Luz CSIC ORCID ; Ramos, Lourdes CSIC ORCID | Fecha de publicación: | 2010 | Editor: | American Chemical Society | Citación: | Journal of Agricultural and Food Chemistry 58(22): 11561-11567 (2010) | Resumen: | A new method based on comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry (GC×GC-ToF MS) has been developed for the first time for the analysis of complex mixtures of disaccharides previously converted to their trimethylsilyl oximes (TMSO). Among the different experimental parameters considered for optimization, both the column set combination and the dimensions of the second-dimension column were found to be the most significant with regard to the complete resolution of structurally similar disaccharides. Application of the optimized method to honey analysis allowed the separation of most of the honey disaccharides previously described in the literature. Furthermore, 12 other unknown disaccharides have been separated by this method and characterized from their mass spectral data. | Versión del editor: | https://doi.org/10.1021/jf102646n | URI: | http://hdl.handle.net/10261/191946 | DOI: | 10.1021/jf102646n | ISSN: | 0021-8561 | E-ISSN: | 1520-5118 |
Aparece en las colecciones: | (IQOG) Artículos |
Ficheros en este ítem:
Fichero | Descripción | Tamaño | Formato | |
---|---|---|---|---|
accesoRestringido.pdf | 59,24 kB | Adobe PDF | Visualizar/Abrir |
CORE Recommender
PubMed Central
Citations
1
checked on 16-abr-2024
SCOPUSTM
Citations
18
checked on 02-may-2024
WEB OF SCIENCETM
Citations
14
checked on 28-feb-2024
Page view(s)
177
checked on 02-may-2024
Download(s)
17
checked on 02-may-2024
Google ScholarTM
Check
Altmetric
Altmetric
Artículos relacionados:
NOTA: Los ítems de Digital.CSIC están protegidos por copyright, con todos los derechos reservados, a menos que se indique lo contrario.