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http://hdl.handle.net/10261/191946
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Campo DC | Valor | Lengua/Idioma |
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dc.contributor.author | Brokl, M. | es_ES |
dc.contributor.author | Soria, Ana C. | es_ES |
dc.contributor.author | Ruiz-Matute, Ana I. | es_ES |
dc.contributor.author | Sanz, M. Luz | es_ES |
dc.contributor.author | Ramos, Lourdes | es_ES |
dc.date.accessioned | 2019-10-01T08:42:36Z | - |
dc.date.available | 2019-10-01T08:42:36Z | - |
dc.date.issued | 2010 | - |
dc.identifier.citation | Journal of Agricultural and Food Chemistry 58(22): 11561-11567 (2010) | es_ES |
dc.identifier.issn | 0021-8561 | - |
dc.identifier.uri | http://hdl.handle.net/10261/191946 | - |
dc.description.abstract | A new method based on comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry (GC×GC-ToF MS) has been developed for the first time for the analysis of complex mixtures of disaccharides previously converted to their trimethylsilyl oximes (TMSO). Among the different experimental parameters considered for optimization, both the column set combination and the dimensions of the second-dimension column were found to be the most significant with regard to the complete resolution of structurally similar disaccharides. Application of the optimized method to honey analysis allowed the separation of most of the honey disaccharides previously described in the literature. Furthermore, 12 other unknown disaccharides have been separated by this method and characterized from their mass spectral data. | es_ES |
dc.description.sponsorship | This work has been funded by projects CTQ2006-14993/BQU (financed by CICYT) and ANALISYC2 (financed by Comunidad de Madrid). M.B. thanks the Consejería de Educación de la Comunidad de Madrid for a predoctoral contract. | es_ES |
dc.language.iso | eng | es_ES |
dc.publisher | American Chemical Society | es_ES |
dc.rights | closedAccess | es_ES |
dc.title | Separation of disaccharides by comprehensive two-dimensional gas chromatography−time-of-flight mass spectrometry. Application to honey analysis | es_ES |
dc.type | artículo | es_ES |
dc.identifier.doi | 10.1021/jf102646n | - |
dc.description.peerreviewed | Peer reviewed | es_ES |
dc.relation.publisherversion | https://doi.org/10.1021/jf102646n | es_ES |
dc.identifier.e-issn | 1520-5118 | - |
dc.contributor.funder | Comisión Interministerial de Ciencia y Tecnología, CICYT (España) | es_ES |
dc.contributor.funder | Comunidad de Madrid | es_ES |
dc.relation.csic | Sí | es_ES |
oprm.item.hasRevision | no ko 0 false | * |
dc.identifier.funder | http://dx.doi.org/10.13039/100012818 | es_ES |
dc.identifier.funder | http://dx.doi.org/10.13039/501100007273 | es_ES |
dc.identifier.pmid | 20973549 | - |
dc.type.coar | http://purl.org/coar/resource_type/c_6501 | es_ES |
item.cerifentitytype | Publications | - |
item.languageiso639-1 | en | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.grantfulltext | none | - |
item.fulltext | No Fulltext | - |
item.openairetype | artículo | - |
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