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Título: | Optimization of the extraction, clean-up and determination of arsenobetaine in manufactured seafood products by coupling liquid chromatography with inductively coupled plasma atomic emission spectrometry |
Autor: | Ybáñez, Nieves; Vélez, Dinoraz CSIC ORCID; Tejedor, Wedleys; Montoro Martínez, Rosa CSIC | Palabras clave: | Arsenobetaine High-performance liquid chromatography Inductively coupled plasma atomic emission spectrometry Manufactured seafood |
Fecha de publicación: | 1995 | Editor: | Royal Society of Chemistry (UK) | Citación: | JAAS - Journal of Analytical Atomic Spectrometry 10: 459-465 (1995) | Resumen: | A study was carried out to develop and optimize a method for determining arsenobetaine (AB) in seafood products by coupling high-performance liquid chromatography (HPLC) with inductively coupled plasma atomic emission spectrometry (ICP-AES). Extraction, clean-up and instrumental determination of AB were established in real samples representative of fish, molluscs and crustaceans. The analytical features of the method are: detection limit, 0.51 μg g-1 As dry mass (dm) or 0.13 μg g-1 As fresh mass (fm); relative standard deviation (n=6), 8% for cockles, 5% for prawns, 4% for sole and 2% for the Canada National Research Council Reference Material, DORM-1 (Dogfish Muscle) (n=3). The percentage recovery for AB is: 87 ± 6 (cockles), 86 ± 2 (sole), 86 ± 9 (prawns). The analysis of DORM-1 provided an AB value of 16.5 ± 0.9 μg g-1 As dm, agreeing with results obtained by other authors using HPLC-ICP-mass spectrometry. | Versión del editor: | http://dx.doi.org/10.1039/JA9951000459 | URI: | http://hdl.handle.net/10261/331232 | DOI: | 10.1039/JA9951000459 | Identificadores: | doi: 10.1039/JA9951000459 issn: 0267-9477 e-issn: 1364-5544 |
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