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Título: | Structural and spectroscopic study of condensed piperidine bicyclanols. 3-Phenethyl-3-azabicyclo[3.2.1]octan-8-α-ol |
Autor: | Gálvez-Ruano, Enrique; Florencio, Feliciana; Sanz-Aparicio, J. CSIC ORCID; Bellanato, Juana CSIC ; García-Ramos, José Vicente CSIC ORCID | Fecha de publicación: | 1989 | Editor: | Elsevier | Citación: | Journal of Molecular Structure 196: 307-316 (1989) | Resumen: | The IR and 1H and 13C NMR spectra of 3-phenethyl-3-azabicyclo[3.2.1]octan-8-α-ol have been studied in several media, and its crystal structure has been determined by X-ray diffraction. The bicyclic system adopts a chair-envelope conformation with both OH and phenethyl groups in equatorial positions with respect to the piperidine ring. The existence of OH⋯N intermolecular hydrogen bonding in the solid state has been revealed by X-ray and IR data. The results obtained are compared with those previously found for the corresponding β-epimer. © 1989. | URI: | http://hdl.handle.net/10261/66790 | DOI: | 10.1016/0022-2860(89)85027-6 | Identificadores: | doi: 10.1016/0022-2860(89)85027-6 issn: 0022-2860 |
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