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Título: | Dalton communication. New diiridium(I) and diiridium(I,III) complexes containing thiolate ligands. Crystal structures of [(cod)Cl(SC6F5)Ir(μ-SC6F5) 2Ir(cod)] and [{Ir(μ-SC6F5)(CO)2}2] (cod = cycloocta-1,5-diene) |
Autor: | Fonseca, Isabel; Hernández, Elisa; Sanz-Aparicio, J. CSIC ORCID; Terreros Ceballos, Pilar CSIC ; Torrens, Hugo | Fecha de publicación: | 1994 | Editor: | Royal Society of Chemistry (UK) | Citación: | Journal of the Chemical Society, Dalton Transactions: 781-783 (1994) | Resumen: | The complex [{Ir(µ-Cl)(cod)}2]1(cod = cycloocta-1,5-diene) was treated with HSR (R = C6F5)–NEt3 to give the dinuclear iridium(I) complex [{Ir(µ-SR)(cod)}2]2 and with HSR only to give a mixture of 2 and the unusual mixed-valence complex [(cod)Cl(SR)Ir(µ-SR)2Ir(cod)]3; complex 2 was treated with CO to yield [{Ir(µ-SR)(CO)2}2]4, the structure of which, together with that of 2, has been characterised by single-crystal X-ray diffraction. | Versión del editor: | http://dx.doi.org/10.1039/DT9940000781 | URI: | http://hdl.handle.net/10261/335079 | DOI: | 10.1039/DT9940000781 | ISSN: | 1472-7773 |
Aparece en las colecciones: | (IQF) Artículos (ICP) Artículos |
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