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Título: | Analysis of triallate residues in cereals and soil by gas chromatography with ion-trap detection |
Autor: | Sánchez-Brunete, C.; Salto, T.; García-Baudín, J. M.; Tadeo Lluch, José Luis | Fecha de publicación: | 1991 | Editor: | Elsevier | Citación: | Journal of Chromatography B 562(1-2): 525-530 (1991) | Resumen: | Triallate residues in barley seedlings and soil samples were determined by gas chromatography with ion-trap detection. Soil was extracted with methanol on a mechanical shaker, and plants were extracted with acetonitrile in a Sorvall homogenizer. After evaporation of the organic solvents, the residue was dissolved in hexane, and plants extracts were cleaned-up on an alumina column. Gas chromatographic analysis was carried out using a BP-1 fused-silica capillary column with helium as carrier gas. To quantitate residues the total-ion chromatogram was obtained and then the selected-ion monitoring chromatograms were displayed at m/z 86 for triallate and at m/z 154 for the internal standard, methyl-(4-amino-2-chloro)-benzoate. The average recovery through the method from barley and soil samples was always higher than 80%. The limit of detection in the selected-ion mode was 0.01 mg/kg. Barley and soil samples treated with triallate were also analysed. A good agreement was observed between results obtained by this method and by gas chromatography with nitrogen-phosphorus detection. © 1991. | URI: | http://hdl.handle.net/10261/291400 | DOI: | 10.1016/0378-4347(91)80604-B | ISSN: | 1570-0232 |
Aparece en las colecciones: | (INIA) Artículos |
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