Por favor, use este identificador para citar o enlazar a este item:
http://hdl.handle.net/10261/192941
COMPARTIR / EXPORTAR:
SHARE BASE | |
Visualizar otros formatos: MARC | Dublin Core | RDF | ORE | MODS | METS | DIDL | DATACITE | |
Título: | In-situ cure monitoring of epoxy/graphene nanocomposites by several spectroscopic techniques |
Autor: | Yuste, Vanesa CSIC; Hernández, Marianella CSIC ORCID ; Ezquerra, Tiberio A. CSIC ORCID; Verdejo, Raquel CSIC ORCID ; López-Manchado, Miguel A. CSIC ORCID | Fecha de publicación: | 2019 | Resumen: | Cure protocols of thermoset resins usually comprise two isothermal steps where resins undergo molecular cross-linking processes. The cure conditions are crucial to ensure a consistent and reliable manufacturing of the piece and have been the subject of an important body of research. While most studies have been carried out by traditional calorimetry or infrared spectroscopy under dynamic conditions, the development of new sensors and in-situ characterization techniques has resulted on a renewed interest on the subject under industrial isothermal protocols. Here, we monitor the curing reaction of both un-filled and nanofilled epoxy resin using broadband dielectric spectroscopy (BDS) and correlate the results with in-situ FT-IR and Raman spectroscopy. Hence, the proposed methodology provides complementary information on the chemical reactions and molecular dynamics associated to the cure cycle and can be an efficient tool for real-time monitorization of thermoset composites manufacturing. | Versión del editor: | http://dx.doi.org/10.1016/j.polymertesting.2019.106114 | URI: | http://hdl.handle.net/10261/192941 | DOI: | 10.1016/j.polymertesting.2019.106114 | Identificadores: | doi: 10.1016/j.polymertesting.2019.106114 issn: 0142-9418 e-issn: 1873-2348 |
Aparece en las colecciones: | (ICTP) Artículos |
Ficheros en este ítem:
Fichero | Descripción | Tamaño | Formato | |
---|---|---|---|---|
Repository_Hernández et al_Polymer Testing.pdf | 1,27 MB | Adobe PDF | Visualizar/Abrir |
CORE Recommender
WEB OF SCIENCETM
Citations
2
checked on 01-dic-2021
Page view(s)
240
checked on 16-may-2024
Download(s)
184
checked on 16-may-2024
Google ScholarTM
Check
Altmetric
Altmetric
NOTA: Los ítems de Digital.CSIC están protegidos por copyright, con todos los derechos reservados, a menos que se indique lo contrario.