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Título: | Pluronic-assisted hydrothermal synthesis of microporous polyimides. Application as supports for heterogenized transition metal catalysts |
Autor: | Rangel-Rangel, E.; González de la Campa, José; Iglesias, Marta CSIC ORCID ; Maya, Eva M. CSIC ORCID; Weber, J. | Palabras clave: | Palladium Hydrothermal synthesis Iron Porous polyimides Heterogenized catalyst |
Fecha de publicación: | 2017 | Editor: | Elsevier | Citación: | Microporous and Mesoporous Materials 239: 287-295 (2017) | Resumen: | Porous polyimides were synthesized fast and easily in water by combining the hydrothermal synthesis with the use of an amphiphilic block copolymer, Pluronic F-127 (HT-PF method) and were fully characterized. Their properties were compared with those of polyimides with the same chemical structure synthesized using m-cresol as solvent and isoquinoline as catalyst. Two of the polyimides synthesized by the HT-PF method were used as supports to obtain heterogenized palladium or iron catalysts (Pd-(HTPF), Fe-(HT-PF); both metal-polyimides showed good catalytic activity Suzuki CeC coupling reactions and alkylation of amines with alcohols, respectively without metal leaching detected during the reaction. | Versión del editor: | http://dx.doi.org/10.1016/j.micromeso.2016.10.029 | URI: | http://hdl.handle.net/10261/155342 | DOI: | 10.1016/j.micromeso.2016.10.029 | Identificadores: | doi: 10.1016/j.micromeso.2016.10.029 issn: 1387-1811 |
Aparece en las colecciones: | (ICTP) Artículos (ICMM) Artículos |
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