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Title

Pluronic-assisted hydrothermal synthesis of microporous polyimides. Application as supports for heterogenized transition metal catalysts

AuthorsRangel-Rangel, E.; González de la Campa, José; Iglesias, Marta ; Maya, Eva M. ; Weber, J.
KeywordsPalladium
Hydrothermal synthesis
Iron
Porous polyimides
Heterogenized catalyst
Issue Date2017
PublisherElsevier
CitationMicroporous and Mesoporous Materials 239: 287-295 (2017)
AbstractPorous polyimides were synthesized fast and easily in water by combining the hydrothermal synthesis with the use of an amphiphilic block copolymer, Pluronic F-127 (HT-PF method) and were fully characterized. Their properties were compared with those of polyimides with the same chemical structure synthesized using m-cresol as solvent and isoquinoline as catalyst. Two of the polyimides synthesized by the HT-PF method were used as supports to obtain heterogenized palladium or iron catalysts (Pd-(HTPF), Fe-(HT-PF); both metal-polyimides showed good catalytic activity Suzuki CeC coupling reactions and alkylation of amines with alcohols, respectively without metal leaching detected during the reaction.
Publisher version (URL)http://dx.doi.org/10.1016/j.micromeso.2016.10.029
URIhttp://hdl.handle.net/10261/155342
DOI10.1016/j.micromeso.2016.10.029
Identifiersdoi: 10.1016/j.micromeso.2016.10.029
issn: 1387-1811
Appears in Collections:(ICTP) Artículos
(ICMM) Artículos
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