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Título: | Syntheses of new titanium(iv) and rhodium(i) guanidinido complexes |
Autor: | Rojas Muñoz, Sergio CSIC ORCID; Otero, Antonio; Rodríguez, Ana CSIC ORCID CVN; Terreros Ceballos, Pilar CSIC | Palabras clave: | N ligands Titanium Rhodium Guanidines Half-sandwich complexes X-ray diffraction |
Fecha de publicación: | 2007 | Editor: | Czech Academy of Sciences | Citación: | Collection of Czechoslovak Chemical Communications 72(4): 579-588 (2007) | Resumen: | The new titanium guanidinido complexes [TiCp*Me2((PhN) 2CNH2)] (1), and [TiCp*Cl2-((PhN) 2CNH2)] (2) (Cp* = η5-C 5Me5) have been synthesized. The reaction of complex 1 with [Rh(n-OH)(cod)]2 affords the rhodium guanidinido complex [Rh{(PhNH)(PhN)CNH}(cod)]2 (3). The molecular structures of complexes 1 and 3 were studied by X-ray diffraction methods. Complex 3 can also be prepared by reaction of [Rh(μ-OH)(cod)]2 with N,N'- diphenylguanidlne. © 2007 Institute of Organic Chemistry and Biochemistry. | Versión del editor: | http://dx.doi.org/10.1135/cccc20070579 | URI: | http://hdl.handle.net/10261/335354 | DOI: | 10.1135/cccc20070579 | ISSN: | 0010-0765 |
Aparece en las colecciones: | (ICP) Artículos |
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