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Título: | Regioselective Enzyme-catalyzed Synthesis of Pyrazole-containing Podands |
Autor: | Flerros, Marta; Rodríguez-Franco, María Isabel CSIC ORCID ; Navarro Torres, Pilar CSIC ; Conde, Santiago CSIC | Fecha de publicación: | 1993 | Editor: | Japan Institute of Heterocyclic Chemistry | Citación: | Heterocycles 36(9): 2019-2034 (1993) | Resumen: | Initial results are described about a new synthesis of a family of the acylic cation-complexing compounds named podands containing a pyrazole moiety as a part of the molecule. This synthesis was carried out by lipase-catalyzed transesterification of the corresponding pyrazole-3,5-dicarbethoxy derivative with di- and triethyleneglycol monomethylether; it afforded good yields and a high degree of regioselectivity in N-substituted pyrazoles where 3 and 5 positions are not equivalents. As an initial approach, a simpler model of transesterification with n-octanol was studied. | Versión del editor: | http://dx.doi.org/10.3987/COM-93-6378 | URI: | http://hdl.handle.net/10261/334169 | DOI: | 10.3987/COM-93-6378 | Identificadores: | doi: 10.3987/COM-93-6378 issn: 1881-0942 |
Aparece en las colecciones: | (IQM) Artículos |
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