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Título: | Preparative HPLC resolution of the cis cyclohexane analogs of phenylalanine |
Autor: | Alías, Miriam CSIC; Cativiela, Carlos CSIC ORCID; Jiménez, Ana I. CSIC ORCID; López, Pilar; Oliveros, Laureano; Marraud, Michel | Fecha de publicación: | 2001 | Editor: | Wiley-VCH | Citación: | Chirality 13(1): 48-55 (2001) | Resumen: | The analytical resolution of different derivatives of cis c6Phe (cyclohexane analogs of phenylalanine) was tested by HPLC using the mixed 10-undecenoate/3,5-dimethylphenylcarbamate of amylose bonded on allylsilica gel as the chiral stationary phase. The same chiral support has allowed the enantioseparation of racemate cis-4 on a semipreparative column (150 × 20 mm ID) with a mixture of n-hexane/2-propanol/chloroform as the mobile phase. Some 200–300 mg of the optically pure enantiomers were isolated and transformed into the N-benzyloxycarbonyl amino acids. The X-ray diffraction structure of (1R;2R)-4 is reported. | Versión del editor: | https://doi.org/10.1002/1520-636X(2001)13:1<48::AID-CHIR10>3.0.CO;2-U | URI: | http://hdl.handle.net/10261/272263 | DOI: | 10.1002/1520-636X(2001)13:1<48::AID-CHIR10>3.0.CO;2-U | ISSN: | 0899-0042 |
Aparece en las colecciones: | (ICMA) Artículos |
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