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13C and 15N NMR chemical shifts of 1-(2′,4′-dinitrophenyl) and 1-(2′,4′,6′- trinitrophenyl) pyrazoles in the solid state and in solution

AuthorsGarcía, M. A.; Claramunt, Rosa M.; Elguero, José CSIC ORCID
Issue Date2008
PublisherJohn Wiley & Sons
CitationMagnetic Resonance in Chemistry 46: 697- 700 (2008)
AbstractThe 13C and 15N CPMAS NMR spectra of 18 pyrazoles substituted at position 1 by dinitrophenyl and trinitrophenyl (picryl) groups have been recorded. To help in the assignments, some of these compounds were studied in DMSO-d6 solution. Phenomena such as the conformation of the N-aryl groups and broadening of splittings due to quadrupolar nuclei are discussed. Copyright © 2008 John Wiley & Sons, Ltd.
Publisher version (URL)http://dx.doi.org/10.1002/mrc.2219
Identifiersdoi: 10.1002/mrc.2219
issn: 0749-1581
issn: 1097-458X
Appears in Collections:(IQM) Artículos
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