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http://hdl.handle.net/10261/64280
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Campo DC | Valor | Lengua/Idioma |
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dc.contributor.author | Flores, Gema | - |
dc.contributor.author | Ruiz del Castillo, M. Luisa | - |
dc.contributor.author | Herraiz Carasa, Marta | - |
dc.date.accessioned | 2013-01-17T10:19:30Z | - |
dc.date.available | 2013-01-17T10:19:30Z | - |
dc.date.issued | 2007 | - |
dc.identifier | doi: 10.1016/j.chroma.2007.01.128 | - |
dc.identifier | issn: 0021-9673 | - |
dc.identifier.citation | Journal of Chromatography A 1153 (1-2): 29- 35 (2007) | - |
dc.identifier.uri | http://hdl.handle.net/10261/64280 | - |
dc.description.abstract | A method based on the use of absorbents as packing materials in the interface of the direct coupling between reversed phase liquid chromatography and gas chromatography (RPLC-GC) is proposed. To that end, a comparative study on different adsorbents and absorbents was carried out. Specifically, Tenax TA and Gaschrom were used as adsorbents while polydimethylsiloxane and poly(50% phenyl:50% methylsiloxane) were the absorbents tested. Some experimental variables involved in the solvent elimination were separately optimised for adsorbent and absorbent materials. Relative standard deviations (RSD) lower than 10% were achieved in all cases but the use of absorbents showed interesting advantages with respect to adsorbents, namely a simpler performance of the experimental work, which facilitates the sample preparation step and the subsequent gas chromatographic analysis to be performed. © 2007 Elsevier B.V. All rights reserved. | - |
dc.language.iso | eng | - |
dc.publisher | Elsevier | - |
dc.rights | closedAccess | - |
dc.subject | On-line coupling RPLC–GC | - |
dc.subject | Absorbents | - |
dc.subject | PTV | - |
dc.title | Absorbents as packing materials in on-line coupling of reversed phase liquid chromatography and gas chromatography via a programmed temperature vaporizer | - |
dc.type | artículo | - |
dc.identifier.doi | 10.1016/j.chroma.2007.01.128 | - |
dc.date.updated | 2013-01-17T10:19:31Z | - |
dc.description.version | Peer Reviewed | - |
dc.type.coar | http://purl.org/coar/resource_type/c_6501 | es_ES |
item.openairetype | artículo | - |
item.grantfulltext | none | - |
item.cerifentitytype | Publications | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.fulltext | No Fulltext | - |
item.languageiso639-1 | en | - |
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accesoRestringido.pdf | 15,38 kB | Adobe PDF | Visualizar/Abrir |
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