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Development of a robust method for the quantitative determination of disaccharides in honey by gas chromatography

AuthorsFuente, Esther de la; Sanz, M. Luz ; Martínez-Castro, Isabel ; Sanz Perucha, Jesús
Issue Date2006
CitationJournal of Chromatography A 1135: 212- 218 (2006)
AbstractAn iterative method for the GC quantitative determination of TMS-oxime disaccharides in honey has been developed. This approach takes into account possible positive systematic errors caused by unidentified compounds which overlap with the expected disaccharides. The results of its application to the determination of 15 disaccharides in simulated honey samples indicate that the iterative method is more robust that methods based on least-squares regression, improves the accuracy of the quantitative analysis and allows to detect the possible presence of disaccharides not identified. © 2006 Elsevier B.V. All rights reserved.
Identifiersdoi: 10.1016/j.chroma.2006.09.035
issn: 0021-9673
e-issn: 1873-3778
Appears in Collections:(IQOG) Artículos
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