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Título: | Characterization of O-trimethylsilyl oximes of trisaccharides by gas chromatography-mass spectrometry |
Autor: | Brokl, M. CSIC; Soria, Ana C. CSIC ORCID ; Martínez-Castro, Isabel CSIC ; Sanz, M. Luz CSIC ORCID ; Ruiz-Matute, Ana I. CSIC ORCID | Fecha de publicación: | 2009 | Editor: | Elsevier | Citación: | Journal of Chromatography A 1216: 4689- 4692 (2009) | Resumen: | Gas chromatography (GC) data (linear retention indices and relative areas) and mass spectra (most representative m/z fragments) of 12 reducing trisaccharides as trimethylsilyl oximes (TMSO) and four non-reducing as trimethylsilyl (TMS) ethers have been described for the first time and related to their structural features. Some trends have been observed: earlier elution of non-reducing compounds and fructotrioses; aldotrioses bearing the reducing end with link in position 6 showing the highest retention. Abundance of several fragment ions and their ratios were useful for trisaccharide characterization; some of these features seem to be useful for the characterization of new trisaccharides. © 2009 Elsevier B.V. All rights reserved. | URI: | http://hdl.handle.net/10261/62722 | DOI: | 10.1016/j.chroma.2009.03.069 | Identificadores: | doi: 10.1016/j.chroma.2009.03.069 issn: 0021-9673 e-issn: 1873-3778 |
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