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Título: | Inclusion of the herbicide 2,4-dichlorophenoxyacetic acid (2,4-D) with β-cyclodextrin by different processing methods |
Autor: | Ginés, J.M.; Pérez-Martínez, José Ignacio CSIC; Arias Blanco, M. J.; Moyano Méndez, José Ramón; Morillo González, Esmeralda CSIC ORCID ; Ruíz-Conde, Antonio; Sánchez-Soto, Pedro José CSIC ORCID | Fecha de publicación: | 1996 | Editor: | Pergamon Press | Citación: | Chemosphere 33(2): 321-334 (1996) | Resumen: | The interaction of the herbicide 2,4-Dichlorophenoxyacetic acid (2,4-D) with β-Cyclodextrin produces the formation of a new inclusion compound in solution and in solid state. XRD, FTIR, DSC and SEM techniques have allowed to investigate the inclusion process of the three processing methods (co-precipitation, spray-drying and kneading) under test. Inclusion of 2,4-D in β-CD in solution was also studied by phase solubility, being determined for the complex an apparent stability constant of 336 M-1. At the solid state, co-precipitation and spray-drying were found to yield an inclusion complex in 1:1 stoichiometry. From these systems, it was attained an increase of 2,4-D aqueous dissolution rate as compared with the uncomplexed herbicide, the spray-dried outcomed being the most effective one. This finding would allow a more rational application of 2,4-D and thus diminish its risks as potential pollutant of ground waters and soils. | URI: | http://hdl.handle.net/10261/62187 | DOI: | 10.1016/0045-6535(96)00175-0 | Identificadores: | doi: 10.1016/0045-6535(96)00175-0 issn: 0045-6535 e-issn: 1879-1298 |
Aparece en las colecciones: | (IRNAS) Artículos (ICMS) Artículos |
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