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dc.contributor.authorAsensio, Gregorio-
dc.contributor.authorEsteruelas, Miguel A.-
dc.contributor.authorOliván, Montserrat-
dc.contributor.authorValencia, Marta-
dc.date.accessioned2012-07-20T11:27:12Z-
dc.date.available2012-07-20T11:27:12Z-
dc.date.issued2010-
dc.identifierdoi: 10.1021/ic101498h-
dc.identifierissn: 0020-1669-
dc.identifiere-issn: 1520-510X-
dc.identifier.citationInorganic Chemistry 49(19): 8665-8667 (2010)-
dc.identifier.urihttp://hdl.handle.net/10261/53657-
dc.description.abstractComplexes OsCl3{dbf(PiPr2)2} [1; dbf(PiPr2)2 = 4,6-bis(diisopropylphosphino)dibenzofuran], OsCl3{xant(PiPr2)2} [2; xant(PiPr2)2 = 9,9-dimethyl-4,5-bis(diisopropylphosphino)xanthene], and OsCl3{xant(PPh2)2} [3; xant(PPh2)2 = 9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene] have been obtained in high yield by the reaction of the corresponding diphosphine with OsCl3·3H2O. The ruthenium(III) counterparts RuCl3{dbf(PiPr2)2} (4), RuCl3{xant(PiPr2)2} (5), and RuCl3{xant(PPh2)2} (6) are similarly obtained from RuCl3·3H2O in moderate yields. The X-ray structures of dbf(PiPr2)2 and complexes 1−3 are also reported.-
dc.description.sponsorshipFinancial support was provided by the Spanish MICINN (Projects CTQ2008-00810 and CTQ2007-65720 and Consolider Ingenio 2010 CSD2007- 00006), Diputación General de Aragón (E35), and the European Social Fund.-
dc.language.isoeng-
dc.publisherAmerican Chemical Society-
dc.rightsclosedAccess-
dc.titleOsmium(III) Complexes with POP Pincer Ligands: Preparation from Commercially Available OsCl3·3H2O and Their X-ray Structures-
dc.typeArtículo-
dc.identifier.doi10.1021/ic101498h-
dc.date.updated2012-07-20T11:27:12Z-
dc.description.versionPeer Reviewed-
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