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Direct transformation of crystalline MoO3 into few-layers MoS2

AuthorsCarrascoso-Plana, Felix; Sanchez-Santolino, Gabriel ; Hsu, Chun-wei; Nemes, Norbert M.; Torres-Pardo, Almudena; Gant, Patricia; Mompean, F. J. ; Kalantar-zadeh, Kourosh; Alonso, J. A. ; García-Hernández, M. ; Frisenda, Riccardo; Castellanos-Gómez, Andrés
Issue Date15-May-2020
PublisherMultidisciplinary Digital Publishing Institute
CitationMaterials 13(10): 2293 (2020)
AbstractWe fabricated large-area atomically thin MoS2 layers through the direct transformation of crystalline molybdenum trioxide (MoO3) by sulfurization at relatively low temperatures. The obtained MoS2 sheets are polycrystalline (~10–20 nm single-crystal domain size) with areas of up to 300 × 300 µm2, 2–4 layers in thickness and show a marked p-type behavior. The synthesized films are characterized by a combination of complementary techniques: Raman spectroscopy, X-ray diffraction, transmission electron microscopy and electronic transport measurements.
Publisher version (URL)https://doi.org/10.3390/ma13102293
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