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Improvements to x-ray diffractometers: Heaters, hygrometry, and thermodifferential and spectra analyses

AutorGarcía-Guinea, Javier ; Ortiz, Ramón ; Correcher, Virgilio; Iglesia, A. la
Fecha de publicaciónoct-2001
EditorAmerican Institute of Physics
CitaciónReview of Scientific Instruments 72(10): 4005 (2001)
ResumenWe describe a newly designed stainless steel door which holds cooling fluids and permits the connection of a set of self-improvements to mechanical supplies, sensors, thermocouples, electronic circuits, and new software to traditional x-ray diffraction chambers. Some compatible analytical routines, at various gas temperatures (from 18 to 200 °C), stem from restricted combinations of stimulation sources to the sample (x irradiation and heating) and the detector sensors (Geiger x-ray diffraction spectra charge coupled devices, humidity, image TV, thermocouples differential thermal analysis installed). Phase transitions of solids can be detected by spectral, structural, geometrical, and thermodifferential methods.
Descripción3 pages, 2 figures, 1 table.
Versión del editorhttp://dx.doi.org/10.1063/1.1403008
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