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Title

Microsize and nanosize BPO4 from pyrolysis of a carborane-substituted polyphosphazene

AuthorsDíaz, Carlos; Jiménez, Josefina ; Laguna, Antonio ; Valenzuela, Maria Luisa
KeywordsPolyphosphazenes
Carborane
Boron
Nanoparticles
Organometallic polymers
Pyrolysis
Issue Date28-Oct-2006
PublisherSpringer
CitationJournal of Inorganic and Organometallic Polymers and Materials 16(3): 211-218 (2006)
AbstractPyrolysis in air of the carborane-substituted polyphosphazene, {[NP({OCH2}2C2B10H10)]0.5 [NP({OCH2}2C2B9H10· NBu4)]0.5} n affords BPO4 crystals of varied sizes in the micro and nano regime.The materials were characterised by IR spectroscopy, SEM-EDAX, TEM, X-ray diffraction, and DTA analysis. A possible mechanism for the formation of these materials is discussed and compared with that found for the formation of metallic nanostructured materials from the pyrolysis of anchored organometallic derivatives of polyphosphazenes.
Description8 pages, 4 figures, 6 scheme.-- et al.
Publisher version (URL)http://dx.doi.org/10.1007/s10904-006-9047-6
URIhttp://hdl.handle.net/10261/19495
DOI10.1007/s10904-006-9047-6
ISSN1574-1443
Appears in Collections:(ICMA) Artículos
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