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Growth of Silicalite-1 by a Method Involving Separation of Reactants.

AuthorsMateo, Ester; Lahoz, Ruth; Fuente, Germán F. de la; Paniagua, Andrés; Coronas, Joaquín; Santamaría, Jesús
Issue Date3-Jan-2007
PublisherAmerican Chemical Society
CitationChem. Mater. 19(3): 594-599 (2007)
AbstractTwo solutions of different concentration (that when mixed give rise to a common zeolite precursor gel) are separated by means of a laser-microperforated, 75 μm thick stainless steel sheet. During the hydrothermal synthesis, reactant diffusion from each side promotes crystallization of well-intergrown silicalite-1 crystals on each microperforation (ca. 80 μm in diameter). This method allows a micrometric control of the growth of the zeolitic material and has important advantages when compared with previous systems.
Description6 pages, 5 figures.
Publisher version (URL)http://dx.doi.org/10.1021/cm062317p
Appears in Collections:(ICMA) Artículos
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