English   español  
Please use this identifier to cite or link to this item: http://hdl.handle.net/10261/191479
Share/Impact:
Statistics
logo share SHARE logo core CORE   Add this article to your Mendeley library MendeleyBASE

Visualizar otros formatos: MARC | Dublin Core | RDF | ORE | MODS | METS | DIDL
Exportar a otros formatos:

Title

Selected standard protocols for the synthesis, phase transfer, and characterization of inorganic colloidal nanoparticles

AuthorsHühn, Jonas; Carrillo-Carrion, Carolina; Soliman, Mahmoud G.; Pfeiffer, Christian; Valdeperez, Daniel; Masood, Atif; Chakraborty, Indranath; Zhu, Lin; Gallego, Marta ; Yue, Zhao; Carril, Monica; Feliu, Neus; Escudero, A. ; Alkilany, Alaaldin. M.; Pelaz, Beatriz.; Pino, Pablo del; Parak, Wolfgang J.
Issue Date10-Jan-2017
PublisherAmerican Chemical Society
CitationChemistry of Materials 29(1): 399-461 (2017)
AbstractSynthesis, characterization, and applications of colloidal nanoparticles have been a prominent topic of current research interests within the last two decades. Available reports in the literature that describe the synthesis of colloidal nanoparticles are abundant with various degrees of reproducibility and simplicity. Moreover, different methods for the characterization of colloidal nanoparticle's basic properties are employed, resulting in conflicting results in many cases. Herein, we describe >in detail> selected standard protocols for the synthesis, purification, and characterization of various types of colloidal inorganic nanoparticles including gold nanoparticles, silver nanoparticles, iron oxide nanoparticles, and quantum dots. This report consists of five main parts: The first and the second parts are dedicated to describing the synthesis of various types of hydrophobic and hydrophilic nanoparticles in organic solvents and in aqueous solutions, respectively. The third part describes surface modification of nanoparticles with a focus on ligand exchange reactions, to allow phase transfer of nanoparticles from aqueous to organic solvents and vice versa. The fourth and the fifth parts describe various general purification and characterization techniques used to purify and characterize nanoparticles, respectively. Collectively, this contribution does not aim to cover all available protocols in the literature to prepare inorganic nanoparticles but rather provides detailed synthetic procedures for important inorganic nanocrystals with a full description of their purification and characterization process.
Publisher version (URL)https://doi.org/10.1021/acs.chemmater.6b04738
URIhttp://hdl.handle.net/10261/191479
DOI10.1021/acs.chemmater.6b04738
ISSN0897-4756
E-ISSN1520-5002
Appears in Collections:(ICMS) Artículos
Files in This Item:
File Description SizeFormat 
accesoRestringido.pdf15,38 kBAdobe PDFThumbnail
View/Open
Show full item record
Review this work
 

Related articles:


WARNING: Items in Digital.CSIC are protected by copyright, with all rights reserved, unless otherwise indicated.