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Intercalated water in multi-layered graphene oxide paper: an X-ray scattering study

AuthorsRouzière, Stéphan; Núñez, Jesús David; Paineau, Erwan; Benito, Ana M. CSIC ORCID ; Maser, Wolfgang K. CSIC ORCID ; Launois, Pascale
KeywordsX-ray scattering modelling
Wide-angle X-ray scattering
Graphene oxide
Issue DateJun-2017
PublisherInternational Union of Crystallography
CitationJournal of Applied Crystallography 50: 876-884 (2017)
AbstractX-ray scattering (XRS) experiments have been performed on multi-layered graphene oxide (GO) paper. GO can be easily hydrated as water naturally intercalates in the hydro­philic nanostructure. The effect of the intercalated water on the XRS signals is measured during dehydration under thermal treatment in the temperature range 298–473 K as well as during hydration under saturated water vapour pressure. A simple modelling of the XRS signals by taking into account the presence and the type of intercalated water (bound water or physisorbed water) is introduced. It allows an explanation of the variations of intensity and position of XRS reflections observed experimentally.
Identifiersdoi: 10.1107/S1600576717006227
issn: 1600-5767
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