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| Título: | Synthesis of a new 24-membered tetramide macrocycle and X-ray crystal structure determination |
Autor: | Santa María, Dolores; Claramunt, Rosa M.; Torralba, M. Carmen; Torres, M. Rosario; Elguero, José CSIC ORCID | Palabras clave: | Macrocycles Inclusion compounds X-ray Amides |
Fecha de publicación: | 2019 | Editor: | Elsevier | Citación: | Tetrahedron Letters 60: 1206-1209 (2019) | Resumen: | The synthesis and characterization of a new 24-membered tetramide macrocycle (6) related to Leigh's macrocycles and catenanes is reported. The replacement of p-xylylenediamine (Leigh) by m-xylylenediamine (this work) strongly modifies the geometry and properties of the new macrocycle. NMR spectroscopy (in DMSO‑d solution) and X-ray crystallography have been used to characterize compound 6. The structural features in the crystal (conformational aspects and H-bonding) have been discussed comparatively to two similar macrocycles NEWHIJ and UJUNOC. | Versión del editor: | http://dx.doi.org/10.1016/j.tetlet.2019.03.066 | URI: | http://hdl.handle.net/10261/184718 | DOI: | 10.1016/j.tetlet.2019.03.066 | Identificadores: | doi: 10.1016/j.tetlet.2019.03.066 issn: 1873-3581 |
| Aparece en las colecciones: | (IQM) Artículos |
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| accesoRestringido.pdf | 15,38 kB | Adobe PDF |  Visualizar/Abrir |
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