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Efficient cycloaddition of arynes to carbon nanotubes under microwave irradiation

AuthorsCriado, A.; Vizuete, María; Gómez-Escalonilla, Maria José; García-Rodríguez, Sergio ; García Fierro, José Luis ; Cobas, Agustín; Peña, Diego; Guitián, Enrique; Langa, Fernando
Issue DateNov-2013
CitationCarbon 63: 140-148 (2013)
AbstractThe functionalization of single-wall carbon nanotubes (SWCNT) by cycloaddition reactions with arynes under microwave irradiation has been studied. The efficiency of the functionalization was monitored by XPS, FTIR and Raman spectroscopies, TGA and HR-TEM. All experimental results point to the formation of SWCNT with a high degree of functionalization, with mass increases ranging from 6.4% to 15.1% depending on the aryne substitution.
Publisher version (URL)https://doi.org/10.1016/j.carbon.2013.06.064
Appears in Collections:(ICP) Artículos
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