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Title

Reduction of aliphatic nitramines. Approach to the synthesis of nitrosamines and amines

AuthorsArmas, Pedro de CSIC; Francisco, Cosme G. CSIC; Hernández, Rosendo CSIC; Suárez, Ernesto CSIC ORCID
Issue Date1986
PublisherElsevier
CitationTetrahedron Letters 27(27): 3195-3198 (1986)
AbstractDeoxygenation of several aliphatic nitramines with tributyltin hydride in the presence of AIBN led to the formation of the corresponding nitrosamines. The nitrosamines underwent denitrosation when submitted to further treatment with tributyltin hydride. The 19-methyl steroid (9) was synthesized by α-alkylation of the nitrosamine (2).
Description4 pages, 2 tables, 2 schemes.
Publisher version (URL)http://dx.doi.org/10.1016/S0040-4039(00)84752-8
URIhttp://hdl.handle.net/10261/17587
DOI10.1016/S0040-4039(00)84752-8
ISSN0040-4039
Appears in Collections:(IPNA) Artículos

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