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http://hdl.handle.net/10261/17249
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Campo DC | Valor | Lengua/Idioma |
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dc.contributor.author | Dorta, Rosa L. | en_US |
dc.contributor.author | Martín, Ángeles | en_US |
dc.contributor.author | Suárez, Ernesto | en_US |
dc.contributor.author | Prangé, Thierry | - |
dc.date.accessioned | 2009-09-29T07:55:12Z | - |
dc.date.available | 2009-09-29T07:55:12Z | - |
dc.date.issued | 1996-07 | en_US |
dc.identifier.citation | Tetrahedron Asymmetry 7(7): 1907-1910 (1996) | en_US |
dc.identifier.issn | 0957-4166 | - |
dc.identifier.uri | http://hdl.handle.net/10261/17249 | - |
dc.description | 4 pages, 1 figure, 2 schemes. | - |
dc.description.abstract | The synthesis of (5R, 7S, 13S)- and (5S, 7S, 13S)-13-methoxy-1,6,8-trioxadispiro[4.1.5.3] pentadecane from tri-O-acetyl-d-glucal, by a convenient homologation of C-1 and C-6 atoms which led to an appropriate dihydroxyl intermediate 7, is reported. The key steps for the construction of the two spiroacetal systems involved a double, step by step, radical abstraction promoted by (diacetoxyiodo)benzene and iodine. | - |
dc.description.sponsorship | This work was supported by the Investigation Programme no. B93-0171 of the Dirección General de Investigación Científica y Técnica and Programmes nos. 93/030 and 93/014 of the Dirección General de Universidades e Investigaci6n del Gobierno de Canarias. A. M. thanks the Ministerio de Educación y Ciencia, Spain, for a fellowship. | - |
dc.format.extent | 2373 bytes | - |
dc.format.extent | 348598 bytes | - |
dc.format.mimetype | text/plain | - |
dc.format.mimetype | application/pdf | - |
dc.language.iso | eng | en_US |
dc.publisher | Elsevier | - |
dc.rights | closedAccess | en_US |
dc.title | Synthesis of (5R, 7S, 13S)-13-methoxy-1,6,8-trioxadispiro[4.1.5.3]pentadecane | en_US |
dc.type | artículo | en_US |
dc.identifier.doi | 10.1016/0957-4166(96)00227-3 | - |
dc.relation.publisherversion | http://dx.doi.org/10.1016/0957-4166(96)00227-3 | - |
dc.contributor.funder | Gobierno de Canarias | - |
dc.contributor.funder | Dirección General de Investigación Científica y Técnica, DGICT (España) | - |
dc.contributor.funder | Ministerio de Educación y Ciencia (España) | - |
dc.identifier.funder | http://dx.doi.org/10.13039/501100008737 | es_ES |
dc.type.coar | http://purl.org/coar/resource_type/c_6501 | es_ES |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.fulltext | No Fulltext | - |
item.cerifentitytype | Publications | - |
item.openairetype | artículo | - |
item.languageiso639-1 | en | - |
item.grantfulltext | none | - |
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