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Título: | Vaccinium meridionale Swartz supercritical CO2 extraction: Effect of process conditions and scaling up |
Autor: | López-Padilla, Alexis CSIC; Ruiz-Rodríguez, Alejandro CSIC ; Restrepo Flórez, Claudia Estela; Rivero Barrios, Diana Marsela; Reglero, Guillermo CSIC ORCID ; Fornari, Tiziana CSIC | Palabras clave: | Scale-up Supercritical fluid extraction Vaccinium meridionale Swartz Extracts |
Fecha de publicación: | 2016 | Editor: | Multidisciplinary Digital Publishing Institute | Citación: | Materials 9(7): 519 (2016) | Resumen: | Vaccinium meridionale Swartz (Mortiño or Colombian blueberry) is one of the Vaccinium species abundantly found across the Colombian mountains, which are characterized by high contents of polyphenolic compounds (anthocyanins and flavonoids). The supercritical fluid extraction (SFE) of Vaccinium species has mainly focused on the study of V. myrtillus L. (blueberry). In this work, the SFE of Mortiño fruit from Colombia was studied in a small-scale extraction cell (273 cm) and different extraction pressures (20 and 30 MPa) and temperatures (313 and 343 K) were investigated. Then, process scaling-up to a larger extraction cell (1350 cm) was analyzed using well-known semi-empirical engineering approaches. The Broken and Intact Cell (BIC) model was adjusted to represent the kinetic behavior of the low-scale extraction and to simulate the large-scale conditions. Extraction yields obtained were in the range 0.1%-3.2%. Most of the Mortiño solutes are readily accessible and, thus, 92% of the extractable material was recovered in around 30 min. The constant CO residence time criterion produced excellent results regarding the small-scale kinetic curve according to the BIC model, and this conclusion was experimentally validated in large-scale kinetic experiments. | Versión del editor: | https://doi.org/10.3390/ma9070519 | URI: | http://hdl.handle.net/10261/150049 | DOI: | 10.3390/ma9070519 | Identificadores: | doi: 10.3390/ma9070519 issn: 1996-1944 |
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