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http://hdl.handle.net/10261/142121
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dc.contributor.author | Ordóñez, Mario | - |
dc.contributor.author | Arizpe, Alicia | - |
dc.contributor.author | Sayago, Francisco J. | - |
dc.contributor.author | Jiménez, Ana I. | - |
dc.contributor.author | Cativiela, Carlos | - |
dc.date.accessioned | 2017-01-04T08:52:02Z | - |
dc.date.available | 2017-01-04T08:52:02Z | - |
dc.date.issued | 2016-08-31 | - |
dc.identifier.citation | Molecules 21(9): 1140 (2016) | - |
dc.identifier.uri | http://hdl.handle.net/10261/142121 | - |
dc.description.abstract | We report here a practical and efficient synthesis of α-aminophosphonic acid incorporated into 1,2,3,4-tetrahydroquinoline and 1,2,3,4-tetrahydroisoquinoline heterocycles, which could be considered to be conformationally constrained analogues of pipecolic acid. The principal contribution of this synthesis is the introduction of the phosphonate group in the N-acyliminium ion intermediates, obtained from activation of the quinoline and isoquinoline heterocycles or from the appropriate δ-lactam with benzyl chloroformate. Finally, the hydrolysis of phosphonate moiety with simultaneous cleavage of the carbamate afforded the target compounds. | - |
dc.description.sponsorship | Financial support to this work was provided by Consejo Nacional de Ciencia y Tecnología (CONACYT-Mexico, grants 181816 and 248868). Ministerio Economia y Competitividad (grant CTQ2013-40855-R), and Gobierno de Aragón-Fondo Social Europeo (research group E40). Consejo Superior de Investigaciones Científicas (grant 2008MX0044). | - |
dc.description.sponsorship | We acknowledge support by the CSIC Open Access Publication Initiative through its Unit of Information Resources for Research (URICI). | - |
dc.publisher | Multidisciplinary Digital Publishing Institute | es_ES |
dc.relation | info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/CTQ2013-40855-R | - |
dc.relation.isversionof | Publisher's version | - |
dc.rights | openAccess | - |
dc.title | Practical and efficient synthesis of α-aminophosphonic acids containing 1,2,3,4-tetrahydroquinoline or 1,2,3,4-tetrahydroisoquinoline heterocycles | - |
dc.type | artículo | - |
dc.identifier.doi | 10.3390/molecules21091140 | - |
dc.relation.publisherversion | http://dx.doi.org/10.3390/molecules21091140 | - |
dc.identifier.e-issn | 1420-3049 | - |
dc.date.updated | 2017-01-04T08:52:03Z | - |
dc.rights.license | http://creativecommons.org/licenses/by/4.0/ | - |
dc.contributor.funder | Consejo Nacional de Ciencia y Tecnología (México) | - |
dc.contributor.funder | Consejo Superior de Investigaciones Científicas (España) | - |
dc.contributor.funder | Ministerio de Economía y Competitividad (España) | - |
dc.contributor.funder | Gobierno de Aragón | - |
dc.contributor.funder | CSIC - Unidad de Recursos de Información Científica para la Investigación (URICI) | - |
dc.identifier.funder | http://dx.doi.org/10.13039/501100003141 | es_ES |
dc.identifier.funder | http://dx.doi.org/10.13039/501100003339 | es_ES |
dc.identifier.funder | http://dx.doi.org/10.13039/501100003329 | es_ES |
dc.identifier.funder | http://dx.doi.org/10.13039/501100010067 | es_ES |
dc.identifier.pmid | 27589713 | - |
dc.type.coar | http://purl.org/coar/resource_type/c_6501 | es_ES |
item.openairetype | artículo | - |
item.grantfulltext | open | - |
item.cerifentitytype | Publications | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.fulltext | With Fulltext | - |
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molecules-21-01140.pdf | 1,28 MB | Adobe PDF | Visualizar/Abrir |
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