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Applicability of Gas Chromatography (GC) Coupled to Triple-Quadrupole (QqQ) Tandem Mass Spectrometry (MS/MS) for Polybrominated Diphenyl Ether (PBDE) and Emerging Brominated Flame Retardant (BFR) Determinations in Functional Foods Enriched in Omega-3

AutorGarcía-Bermejo, Ángel ; Mohr, Susana; Herrero, Laura ; González, María José; Gómara, Belén
Palabras claveOmega-3
Emerging brominated flame retardants
Functional foods
Polybrominated diphenyl ethers
Triple-quadrupole mass spectrometry
Gas chromatography
Fecha de publicación2016
EditorAmerican Chemical Society
CitaciónJournal of agricultural and food chemistry 64: 7265-7274 (2016)
ResumenThis paper reports on the optimization, characterization, and applicability of gas chromatography coupled to triple-quadrupole tandem mass spectrometry (GC-QqQ(MS/MS)) for the determination of 14 polybrominated diphenylethers (PBDEs) and 2 emerging brominated flame retardants, 1,2-bis(2,4,6-tribromophenoxy)ethane (BTBPE) and decabromodiphenylethane (DBDPE), in functional food samples. The method showed satisfactory precision and linearity with instrumental limits of detection (iLODs) ranging from 0.12 to 7.1 pg, for tri- to octa-BDEs and BTBPE, and equal to 51 and 20 pg for BDE-209 and DBDPE, respectively. The highest ΣBFR concentrations were found in fish oil supplements (924 pg/g fresh weight, fw), followed by biscuits (90 pg/g fw), vegetable oil supplements (46 pg/g fw), chicken eggs (45 pg/g fw), cow's milk (7.7 pg/g fw), and soy products (1.6 pg/g fw). BDE-47, BDE-99, and DBDPE were the most abundant compounds. Foodstuffs enriched with omega-3 presented concentrations similar to or even lower than those of conventional foods commercialized in Spain since 2000.
Versión del editorhttp://dx.doi.org/10.1021/acs.jafc.6b03118
URIhttp://hdl.handle.net/10261/140608
DOI10.1021/acs.jafc.6b03118
Identificadoresdoi: 10.1021/acs.jafc.6b03118
issn: 0021-8561
e-issn: 1520-5118
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