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Applications of sample-controlled thermal analysis (SCTA) to kinetic analysis and synthesis of materials

AutorPérez-Maqueda, Luis A. ; Criado Luque, J.M. ; Sánchez-Jiménez, P.E. ; Diánez, M. J.
Fecha de publicación2015
EditorAkadémiai Kiadó (Budapest)
CitaciónJournal of Thermal Analysis and Calorimetry 120: 45- 51 (2015)
ResumenThe advantages of the sample-controlled thermal analysis (SCTA) for both the kinetic analysis of solid-state reactions and the synthesis of materials are reviewed. This method implies an intelligent control of the temperature by the solid-state reaction under study in such a way that the reaction rate as a function of the time fits a profile previously defined by the user. It has been shown that SCTA has important advantages for discriminating the kinetic model of solid-state reactions as compared with conventional rising temperature methods. Moreover, the advantages of SCTA methods for synthesising materials with controlled texture and structure are analysed.
URIhttp://hdl.handle.net/10261/124707
DOI10.1007/s10973-014-4176-6
Identificadoresdoi: 10.1007/s10973-014-4176-6
issn: 1388-6150
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