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Título

Trace-level determination of pharmaceutical residues by LC-MS/MS in natural and treated waters. A pilot-survey study

Autor Hernando, María Dolores; Heath, E.; Petrovic, Mira; Barceló, Damià
Palabras clave Pharmaceuticals
Natural water
Treated water
Liquid chromatography
Tandem mass spectrometry
Fecha de publicación 1-jul-2006
EditorSpringer
Citación Analytical and Bioanalytical Chemistry 385(6):985-991(2006)
ResumenA pilot-survey study was performed by collecting samples (influent and effluent wastewaters, rivers and tap waters) from different locations in Europe (Spain, Belgium, Germany and Slovenia). A solid-phase extraction (SPE) followed by liquid chromatography–tandem mass spectrometry method was applied for the determination of pharmaceuticals (ibuprofen, naproxen, ketoprofen, diclofenac and clofibric acid). Method detection limits and method quantification limits were at the parts-per-trillion level (7.5–75 ng/L). The recovery rates of the SPE from deionized water and effluent wastewater samples spiked at 100- and 1,000-ng/L levels ranged from 87 to 95%. Identification criteria in compliance with the EU regulation for confirmatory methods of organic residues were applied. A detailed study of signal suppression evaluation for analysis of pharmaceutical residues in effluent wastewaters is presented
Descripción 7 pages, 3 tables, 2 figures.
Versión del editorhttp://dx.doi.org/10.1007/s00216-006-0394-5
URI http://hdl.handle.net/10261/11806
DOI10.1007/s00216-006-0394-5
ISSN1618-2642 (Print)
1618-2650 (Online)
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