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Novel PTM-TEMPO biradical for fast dissolution dynamic nuclear polarization

AuthorsMuñoz Gómez, José L.; Marín-Montesinos, Ildefonso; Lloveras, Vega ; Pons, Miquel; Vidal Gancedo, José ; Veciana, Jaume
Issue Date17-Oct-2014
PublisherAmerican Chemical Society
CitationOrganic Letters 16(20): 5402- 5405 (2014)
Abstract© 2014 American Chemical Society. The synthesis and characterization of a novel trityl-TEMPO biradical and the investigation of its properties as Dynamic Nuclear Polarization (DNP) polarizing agent are reported. Comparison with a structurally related monoradical (PTM-TEMPE) or mixtures of the two monoradical components reveals that the biradical has a much higher polarization efficiency and a faster polarization buildup. This o ffers the possibility of faster recycling further contributing to its efficiency as a polarizing agent. (Graph Presented).
Identifiersdoi: 10.1021/ol502644x
e-issn: 1523-7052
issn: 1523-7060
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