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Title

Crystallization and preliminary X-ray analysis of the antimalarial and cytotoxic alkaloid cryptolepine complexed with the DNA fragment d(CCTAGG)2

AuthorsLisgarten, John N.; Pous, Joan ; Coll, Miquel ; Wright, Colin W.; Aymamí, Joan
Issue DateFeb-2002
PublisherBlackwell Publishing
CitationActa Crystallographica. Section D: Biological Crystallography 58(2): 312-313 (2002)
AbstractCrystals of the indoloquinoline alkaloid cryptolepine complexed with the DNA fragment d(CCTAGG)2 have been grown by the hanging-drop technique at 293 K using ammonium sulfate as the precipitating agent. Over a period of three weeks, yellow tapering bullet-shaped crystals grew to maximum dimensions of 0.2 × 0.1 × 0.1 mm. The crystals belong to space group P64, with unit-cell parameters a = b = 29.960, c = 39.64 Å, α = β = 90, γ = 120°, and diffract to 1.4 Å.
Publisher version (URL)http://dx.doi.org/10.1107/S0907444901018960
URIhttp://hdl.handle.net/10261/108281
DOIhttp://dx.doi.org/10.1107/S0907444901018960
Identifiersdoi: 10.1107/S0907444901018960
issn: 0907-4449
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