2024-03-28T18:28:26Zhttp://digital.csic.es/dspace-oai/requestoai:digital.csic.es:10261/19782016-08-09T10:03:25Zcom_10261_33com_10261_5col_10261_286
2007-11-08T17:01:20Z
urn:hdl:10261/1978
A study of polymer-supported bases for the solution phase synthesis of glycosyl trichloroacetimidates
Chiara, José Luis
Encinas, Lourdes
Díaz, Beatriz
Carbohydrates
Solid-supported reagents
Glycosylation
Polystyrene-supported strong organic bases are highly efficient reagents for the solution-phase synthesis of glycosyl trichloroacetimidates, affording quantitative yields of pure products in short reaction times after simple filtration and evaporation. Although efficiency of the different bases varies with substrate structure, polymer-bound 1,8-diazabicyclo[5.4.0]undec-7-ene was found to give the best results for all substrates tested.
2007-11-08T17:01:20Z
2007-11-08T17:01:20Z
2005-04-04
artículo
Tetrahedron Letters 46, 14 (2005), pp. 2445-2448
0040-4039
http://hdl.handle.net/10261/1978
10.1016/j.tetlet.2005.02.055
eng
closedAccess
Elsevier