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Título: | A versatile, non-biomimetic route to the preussomerins: syntheses of (±)-preussomerins F,K and L |
Autor: | Quesada, Ernesto CSIC ORCID ; Stockley, Martin; Ragot, Jacques P.; Prime, Michael E.; Whitwood, Adrian C.; Taylor, Richard J. K. | Fecha de publicación: | 9-ago-2004 | Editor: | Royal Society of Chemistry (UK) | Citación: | Organic & Biomolecular Chemistry 2 (17) : 2483-2495 (2004) | Resumen: | The first total syntheses of the title fungal metabolites preussomerins F, K and L are described and their structures confirmed thereby. The syntheses were achieved following a versatile, unified, non-biomimetic approach, which is easily extendable to prepare other known and novel members of this family. Key steps include the functionalisation of a 2-arylacetal anion, tandem one-pot Friedel–Crafts cyclisation–deprotection, regioselective substrate-directable hydrogenation and reductive-opening of epoxides. | Versión del editor: | http://dx.doi.org/10.1039/B407895K | URI: | http://hdl.handle.net/10261/96431 | DOI: | 10.1039/B407895K | ISSN: | 1477-0520 | E-ISSN: | 1477-0539 |
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