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dc.contributor.authorBlasco, Cristina-
dc.contributor.authorPicó, Yolanda-
dc.contributor.authorAndreu Pérez, V.-
dc.date.accessioned2012-04-03T11:25:28Z-
dc.date.available2012-04-03T11:25:28Z-
dc.date.issued2009-05-
dc.identifier.citationElectrophoresis 30(10): 1698-1707 (2009)es_ES
dc.identifier.issn0173-0835-
dc.identifier.urihttp://hdl.handle.net/10261/47894-
dc.description10 páginas, 2 figuras, 4 tablas.es_ES
dc.description.abstractThis study reports a method based on CE-MS/MS detection developed for the multi-residue determination of seven pesticides (amidosulfuron, cyprodinil, cyromazine, imazaquin, pirimicarb, demethyl pirimicarb, procymidone) and eight residues of veterinary drugs (ciprofloxacin, enrofloxacin, sulfacetamide, sulfabenzamide, sulfachlorpyridazine, sulfaquinoxaline, sulfathiazole, sulfisoxazole), whose contents are regulated by the EU Council Regulations no. 396/2005 and no. 2377/90, in animal edible tissues. Milk samples were extracted with ACN and the extract was cleaned up using an Oasis hydrophilic-lipophilic balance SPE cartridge. The proposed method was validated in accordance with the European Commission Decision 657/2002. MS/MS experiments, using an IT analyzer, operating in multiple reaction monitoring mode, were carried out to achieve the minimum number of required identification points. Recovery data were also satisfactory, with values higher than 78% for most pesticides and veterinary drugs extracted from milk spiked at half the maximum residue limit established for the studied compounds. The RSD% (n = 5) were lower than 13 and 15% for intra-day and inter-day assays, respectively. The method was applied to establish the occurrence of the studied pesticides in 100 milk samples, attaining the determination of pesticide and veterinary drug residues in milk in the low mu g/kg range.es_ES
dc.description.sponsorshipThis work was partially supported by the Conselleria de Sanitat of the Generalitat Valenciana through the projects of research in programmes of Health, Prevention and Prediction of Illness (Project No. 017/2007). The authors have declared no conflict of interest.es_ES
dc.language.isoenges_ES
dc.publisherWiley-VCHes_ES
dc.rightsclosedAccesses_ES
dc.subjectCE-MS/MSes_ES
dc.subjectFoodes_ES
dc.subjectMilkes_ES
dc.subjectPesticideses_ES
dc.subjectVeterinary drugses_ES
dc.titleAnalytical method for simultaneous determination of pesticide and veterinary drug residues in milk by CE-MSes_ES
dc.typeartículoes_ES
dc.identifier.doi10.1002/elps.200800696-
dc.description.peerreviewedPeer reviewedes_ES
dc.relation.publisherversionhttp://dx.doi.org/10.1002/elps.200800696es_ES
dc.contributor.funderGeneralitat Valenciana-
dc.identifier.funderhttp://dx.doi.org/10.13039/501100003359es_ES
dc.type.coarhttp://purl.org/coar/resource_type/c_6501es_ES
item.openairetypeartículo-
item.cerifentitytypePublications-
item.languageiso639-1en-
item.grantfulltextnone-
item.openairecristypehttp://purl.org/coar/resource_type/c_18cf-
item.fulltextNo Fulltext-
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