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3-(Piperidin-1-ium-1-yl)-6-azoniaspiro­[5.5]undecane dibromide monohydrate

AuthorsGonzález, Jorge; Atilano-Coral, Roberto; Peraza-Campos, Ana Lilia; Ortegón-Reyna, David; Álvarez, Eleuterio
KeywordsCrystal structure
Single-crystal X-ray study
Hydrogen bonds
Issue Date7-May-2011
PublisherInternational Union of Crystallography
CitationActa Crystallographica - Section E - Structure Reports Online 67(6): o1308-o1309 (2011)
AbstractThe title compound, C15H30N2 2+·2Br−·H2O, was synthesized by reaction of 4-piperidino­piperidine with dibromo­pentane. The dication is built up from three linked piperidine rings, two of which have one quaternary N atom in common (azoniaspiro), whereas the third is N—C bonded to the azoniaspiro system and protonated on the N atom (piperidinium). All three piperidine rings adopt chair conformations. The crystal structure features O—HBr and N—HBr hydrogen bonds.
Description12 páginas, 2 figuras, tablas.
Publisher version (URL)http://dx.doi.org/10.1107/S1600536811008713
Appears in Collections:(IIQ) Artículos
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