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Title

Method for crystallisation from a solution

AuthorsOsuna-Esteban, Susana ; Zorzano, María Paz ; Menor-Salván, César ; Ruiz Bermejo, Marta ; Veintemillas-Verdaguer, S.
Issue Date3-Mar-2010
CitationEP2169094 A1
AbstractThe present invention relates to a novel method and to a device for obtaining crystals from a substance, comprising: (i) preparing a saturated dissolution of the substance to be crystallized in a suitable solvent in a reaction vessel; (ii) generating an aerosol in the reaction vessel; (iii) crystallizing the substance; and (iv) recovering the crystals at the bottom of the reaction vessel. The method is especially suitable for crystallizing substances which are typically difficult to crystallize and can lead to a chiral amplification result.
La presente invención relaciona a un nuevo método y a un dispositivo para obtener los cristales de una sustancia, comprendiendo: (i) preparando una disolución saturada de la sustancia que se cristalizará en un disolvente adecuado en un recipiente de reacción (ii) generar un aerosol en el recipiente de reacción (iii) cristalizar la sustancia y (iv) recuperando los cristales en el fondo del recipiente de reacción. El método es especialmente adecuado para cristalizar las sustancias que el son típicamente difícil cristalizar y el bote conducen a un resultado de la amplificación del quiral.
URIhttp://hdl.handle.net/10261/28289
Appears in Collections:(ICMM) Patentes
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