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Título: | X-ray absorption spectroscopy investigation on the structure of methyl acrylate-TiCl4 complexes in solution |
Autor: | Assfeld, Xavier; García, Joaquín CSIC ORCID; García, José I. CSIC ORCID ; Mayoral, José A. CSIC ORCID; Proietti, M. G. CSIC ORCID; Ruiz-López, Manuel F.; Sánchez, María Concepción CSIC ORCID | Fecha de publicación: | 1994 | Editor: | Royal Society of Chemistry (UK) | Citación: | Journal of the Chemical Society, Chemical Communications (18): 2165-2166 (1994) | Resumen: | EXAFS and XANES spectra of methyl acrylate–TiCl4 complexes in nitrobenzene show that the titanium atom is coordinated to two oxygen atoms and four chlorine atoms for any methyl acrylate/TiCl4 ratio; furthermore, there is no free TiCl4, so some carbonyls must be coordinated to two titanium atoms, as confirmed by IR spectroscopy; coordination increases the titanium–chlorine distance with regard to TiCl4. | Versión del editor: | https://doi.org/10.1039/C39940002165 | URI: | http://hdl.handle.net/10261/272982 | DOI: | 10.1039/C39940002165 | ISSN: | 0022-4936 |
Aparece en las colecciones: | (ICMA) Artículos |
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