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Título: | Combinatorial Screening of Cuprate Superconductors by Drop-On-Demand Inkjet Printing |
Autor: | Queraltó, Albert CSIC ORCID; Banchewski, Juri CSIC; Pacheco, Adrià; Gupta, Kapil; Saltarelli, Lavinia; García Franco, Diana; Alcalde, Núria; Cristian Mocuta,; Ricart, Susagna CSIC ORCID; Pino, Flavio CSIC ORCID; Obradors, Xavier CSIC ORCID; Puig Molina, Teresa CSIC ORCID | Palabras clave: | Combinatorial chemistry High-throughput experimentation Superconducting materials Inkjet printing Transient liquid-assisted growth Cuprate superconductors Chemical solution deposition |
Fecha de publicación: | 24-feb-2021 | Editor: | American Chemical Society | Citación: | ACS Applied Materials and Interfaces 13(7): 9101–9112 (2021) | Resumen: | Combinatorial and high-throughput experimentation (HTE) is achieving more relevance in material design, representing a turning point in the process of accelerated discovery, development, and optimization of materials based on data-driven approaches. The versatility of drop-on-demand inkjet printing (IJP) allows performing combinatorial studies through fabrication of compositionally graded materials with high spatial precision, here by mixing superconducting REBCO precursor solutions with different rare earth (RE) elements. The homogeneity of combinatorial Y1−xGdxBa2Cu3O7 samples was designed with computational methods and confirmed by energy-dispersive Xray spectroscopy (EDX) and high-resolution X-ray diffraction (XRD). We reveal the advantages of this strategy in the optimization of the epitaxial growth of high-temperature REBCO superconducting films using the novel transient liquid-assisted growth method (TLAG). Advanced characterization methods, such as in situ synchrotron growth experiments, are tailored to suit the combinatorial approach and demonstrated to be essential for HTE schemes. The experimental strategy presented is key for the attainment of large datasets for the implementation of machine learning backed material design frameworks. | Versión del editor: | http://dx.doi.org/10.1021/acsami.0c18014 | URI: | http://hdl.handle.net/10261/235069 | ISSN: | 1944-8244 |
Aparece en las colecciones: | (ICMAB) Artículos |
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