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Title

Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters

AuthorsHayati, Payam ; Suárez-García, Salvio ; Gutiérrez, Angel; Ruiz Molina, Daniel ; Morsali, Ali; Reza Rezvani, Ali
Issue Date2018
PublisherElsevier
CitationUltrasonics Sonochemistry 42: 320-326 (2018)
AbstractOne new lead(II) coordination supramolecular complex (CSC) (1D), [Pb2(L)2(I)4]n, L  =  C4H6N2 (1-methyl imidazole), has been synthesized under different experimental conditions. Micrometric crystals (bulk) or nano-sized materials have been obtained depending on using the branch tube method or sonochemical irradiation. All materials have been characterized by scanning electron microscopy (SEM), powder X-ray diffraction (PXRD) and FT-IR spectroscopy. Single crystal X-ray analyses on complex 1 showed that Pb2+ ion is 4-coordinated. Topological analysis shows that the complex 1 is 2,3,5C2 net. Finally, the role of reaction time and temperature on the growth and final morphology of the structures obtained by sonochemical irradiation have been studied.
Publisher version (URL)https://doi.org/10.1016/j.ultsonch.2017.11.033
URIhttp://hdl.handle.net/10261/199832
DOI10.1016/j.ultsonch.2017.11.033
ISSN1350-4177
E-ISSN1873-2828
Appears in Collections:(CIN2) Artículos
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