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Título: | Mechanically induced combustion synthesis of niobium carbonitride nanoparticles |
Autor: | Jalaly, Maisam; Gotor, F.J. CSIC ORCID ; Sayagués, María Jesús CSIC ORCID | Palabras clave: | Combustion Mechanosynthesis Niobium carbonitride |
Fecha de publicación: | nov-2018 | Editor: | Elsevier | Citación: | Journal of Solid State Chemistry 267: 106-112 (2018) | Resumen: | Niobium carbonitride [Nb(C,N)] nanoparticles were synthesized by a combustive mechanochemical reaction in the Mg/Nb2O5/C3H6N6 system. High-energy ball milling was used to promote a mechanically induced self-sustaining reaction (MSR). Combustion occurred after a very short milling period of 5 min. X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), energy-dispersive X-ray spectroscopy (EDS) and electron energy loss spectroscopy (EELS) analyses revealed that the nature of the product is an intermixed carbonitride material. The formation mechanism of Nb(C,N) resulted from the magnesiothermic reduction of niobium oxide to generate elemental Nb, which then reacted with the species generated from the melamine decomposition. | Versión del editor: | https://doi.org/10.1016/j.jssc.2018.08.027 | URI: | http://hdl.handle.net/10261/194095 | DOI: | 10.1016/j.jssc.2018.08.027 | ISSN: | 0022-4596 |
Aparece en las colecciones: | (ICMS) Artículos |
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