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Title

Lipase-catalysed selective monoacylation of 1,n-diols with vinyl acetate

AuthorsFramis, Victoria; Camps Díez, Francisco ; Clapés Saborit, Pere
KeywordsSymmetric diols
Lipases
Selective monoacetylation
Issue Date21-May-2004
PublisherElsevier
CitationTetrahedron Letters 45(26): 5031-5033 (2004)
AbstractA simple enzymatic methodology for the selective monoacetylation of 1,n-diols (n=5,8) using vinyl acetate is reported. Monoacetylation excesses of 81–87% at 74–90% 1,n-diol conversions were obtained in toluene and diisopropyl ether using Thermomyces lanuginosus lipase (TLL) immobilised on polypropylene powder as catalyst.
A simple enzymatic methodology for the selective monoacetylation of 1,n-diols (n=5,8) using immobilised Thermomyces lanuginosus lipase in different organic media is reported.
Description3 pages, 1 figure, 2 tables.-- Printed version published Jun 21, 2004.
Publisher version (URL)http://dx.doi.org/10.1016/j.tetlet.2004.05.001
URIhttp://hdl.handle.net/10261/18195
DOI10.1016/j.tetlet.2004.05.001
ISSN0040-4039
Appears in Collections:(IQAC) Artículos
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