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Title: | Structure refinement of samarium monothio oxide |
Authors: | Llanos, Jaime; Mújica, Carlos; Henríquez, Alicia; Gómez-Romero, P. CSIC ORCID ; Molins, Elies CSIC ORCID | Keywords: | Inorganic compounds Thiooxides Chemical synthesis X-ray diffraction |
Issue Date: | 2-Mar-2001 | Publisher: | Elsevier | Citation: | Journal of Alloys and Compounds 316(1-2): 90-92 (2001) | Abstract: | The crystal structure of samarium monothio sulfide, was solved using single crystal refined data. Sm2O2S, crystallizes in the trigonal system with space group P m1 (no. 164), Z=1 and cell constants a=388.7(1) pm and c=670.9(3) pm. The discrepancy indices of the single crystal structure refinement were R1=0.031 and wR2=0.077. Sm2O2S is isostructural with M2O2S (M=La, Ce, Nd, and Tm). The structure can be described as a packing of S−2 and O−2 anions with Sm+3 located in the center of a capped octahedron in which the seventh ligand (an oxygen atom) has been added to the triangular face formed only by O atoms. | Publisher version (URL): | http://dx.doi.org/10.1016/S0925-8388(00)01510-3 | URI: | http://hdl.handle.net/10261/15756 | DOI: | 10.1016/S0925-8388(00)01510-3 | ISSN: | 0925-8388 |
Appears in Collections: | (ICMAB) Artículos |
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