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Methyl 1,2-Orthoesters in Acid-Washed Molecular Sieves Mediated Glycosylations

AuthorsUriel, Clara ; Rijo, Patricia; Fernandes, Ana S.; Gómez, Ana M. ; Fraser-Reid, B.; López, J. Cristobal
KeywordsAcid-washed molecular sieves
Methyl orthoesters
Issue Date2016
PublisherChemPubSoc Europe
CitationChemistrySelect 1: 6011-6015 (2016)
AbstractGlycosylation of alcohol derivatives with D-mannose and D- glucose derived methyl 1,2-orthobe nzoates can be promoted by commercially available acid-washed 300 molecular sieves (AW-MS), which functions both as promoter and as a drying agent in an operationally simple process. In this manner, glycosides can be obtained in good to excellent yields at room temperature, reflux, or under microwave (MW) heating. The usefulness of the process has been shown with the prepar ation of some diterpene glycosides.
Publisher version (URL)http://dx.doi.org/10.1002/slct.201601613
Identifiersdoi: 10.1002/slct.201601613
issn: 2365-6549
Appears in Collections:(IQOG) Artículos
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