English   español  
Please use this identifier to cite or link to this item: http://hdl.handle.net/10261/147557
logo share SHARE logo core CORE   Add this article to your Mendeley library MendeleyBASE

Visualizar otros formatos: MARC | Dublin Core | RDF | ORE | MODS | METS | DIDL
Exportar a otros formatos:


Characterization of cyclitol glycosides by gas chromatography coupled to mass spectrometry

AuthorsRuiz Aceituno, Laura ; Carrero-Carralero, Cipriano ; Ruiz-Matute, Ana Isabel; Ramos, Lourdes ; Sanz, M. Luz ; Martínez-Castro, Isabel
KeywordsGas chromatography-mass spectrometry
Adzuki bean
Issue Date2017
CitationJournal of chromatography. A 1484: 58-64 (2017)
AbstractSeveral cyclitol glycosides have been characterised as trimethylsilyl derivatives by their gas chromatographic (GC) retention data (linear retention indices) and electron impact mass spectrometric (MS) profiles. Both GC–MS results have been related to cyclitol glycosides structural features. Abundance ratios of characteristic m/z ions 133/129 and 260/265 have been proposed to distinguish glycosyl-inositols from glycosyl-methyl-inositols. These ratios in combination with the presence or absence of m/z 375 ion allowed the unequivocal characterization of cyclitol glycosides. These criteria have been applied to the characterization of new cyclitol glycosides in chickpea (Cicer arietinum) and adzuki bean (Vigna angularis) and in leaves of Coriaria myrtifolia and Coriaria ruscifolia.
DescriptionSupplementary data associated with this article can be found, in the online version, at http://dx.doi.org/10.1016/j.chroma.2017.01. 001.
Publisher version (URL)http//dx.doi.org/10.1016/j.chroma.2017.01.001
Identifiersdoi: 10.1016/j.chroma.2017.01.001
issn: 0021-9673
e-issn: 1873-3778
Appears in Collections:(IQOG) Artículos
Files in This Item:
File Description SizeFormat 
accesoRestringido.pdf15,38 kBAdobe PDFThumbnail
Show full item record
Review this work

Related articles:

WARNING: Items in Digital.CSIC are protected by copyright, with all rights reserved, unless otherwise indicated.