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| Title: | Intramolecular 1,5-hydrogen atom transfer reaction promoted by phosphoramidyl and carbamoyl radicals: synthesis of 2-amino-C-glycosides |
Authors: | Francisco, Cosme G. CSIC; Herrera, Antonio J. CSIC ; Martín, Ángeles CSIC ORCID ; Pérez-Martín, Inés CSIC ORCID ; Suárez, Ernesto CSIC ORCID | Issue Date: | 4-Jul-2007 | Publisher: | Elsevier | Citation: | Tetrahedron Letters 48(36): 6384-6388 (2007) | Abstract: | The preparation of 2-amino-C-glycosides of the hexahydro-2H-furo[3,2-b]pyrrole and octahydropyrano[3,2-b]pyrrole systems is described. A tandem 1,5-hydrogen atom transfer–radical oxidation–nucleophilic cyclisation mechanism is proposed for the intramolecular hydrogen atom transfer reaction promoted by carbamoyl and phosphoramidyl radicals employing hipervalent iodine oxidants. | Description: | 5 páginas, 2 tablas, 3 esquemas. Full characterisation of compounds and experimental details. Supplementary data (13 pages) available at: http://dx.doi.org/10.1016/ j.tetlet.2007.06.152 |
Publisher version (URL): | http://dx.doi.org/10.1016/j.tetlet.2007.06.152 | URI: | http://hdl.handle.net/10261/12979 | DOI: | 10.1016/j.tetlet.2007.06.152 | ISSN: | 0040-4039 |
| Appears in Collections: | (IPNA) Artículos |
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| File | Description | Size | Format | |
|---|---|---|---|---|
| TL 2007 48 6384.pdf | Artículo principal | 1,48 MB | Adobe PDF |  View/Open |
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