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Title

Rapid, efficient and solvent free microwave mediated synthesis of aldo- and ketonitrones

AuthorsMaiuolo, Loredana; Nino, Antonio de; Merino, Pedro ; Russo, Beatrice; Stabile, Gaetano; Nardi, Monica; D'Agostino, Napoleone; Bernardi, Beatrice
KeywordsNitrones
Microwaves
Issue Date2015
PublisherElsevier
CitationArabian Journal of Chemistry 9(1): 25-31 (2015)
AbstractA library of C-alkyl and C-aryl nitrones has been obtained by direct condensation of primary N-substituted hydroxylamine hydrochlorides with various aldehydes and ketones without catalysts or base. The synthetic procedure, performed under MW irradiation in the absence of solvent, does not require the presence of a base, is fast, clean, high-yielding and characterized by simple work-up.
DescriptionUnder a Creative Commons license.
Publisher version (URL)http://dx.doi.org/10.1016/j.arabjc.2015.01.015
URIhttp://hdl.handle.net/10261/122608
DOI10.1016/j.arabjc.2015.01.015
ISSN1878-5352
Appears in Collections:(ISQCH) Artículos
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