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http://hdl.handle.net/10261/115642
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dc.contributor.author | Vargas-Becerril, Nancy | - |
dc.contributor.author | Téllez-Jurado, Lucía | - |
dc.contributor.author | Reyes-Gasga, J. | - |
dc.contributor.author | Alvarez-Perez, M. A. | - |
dc.contributor.author | Rodríguez-Lorenzo, Luis M. | - |
dc.date.accessioned | 2015-05-22T10:38:09Z | - |
dc.date.available | 2015-05-22T10:38:09Z | - |
dc.date.issued | 2014 | - |
dc.identifier | doi: 10.1007/s10971-014-3478-2 | - |
dc.identifier | issn: 0928-0707 | - |
dc.identifier | e-issn: 1573-4846 | - |
dc.identifier.citation | Journal of Sol-Gel Science and Technology 72: 571-580 (2014) | - |
dc.identifier.uri | http://hdl.handle.net/10261/115642 | - |
dc.description.abstract | Pechini method is a materials synthesis method based on the preparation of a polymeric matrix. The advantage of this method is the ability to obtain materials with different particle sizes depending on the synthesis condition with a homogeneous distribution. In this work, carbonated hydroxyapatite (c-OHAp) nanoparticles were obtained by a modified Pechini method. To obtain the polymeric precursor of the c-OHAp, the polymeric matrix was prepared through a polyesterification reaction between citric acid and ethylene-glycol. Adding calcium hydroxide and ortophosphoric acid in aqueous solutions, raising the temperature up to 140 C/2 h and keeping constant the pH at 8. The polymeric matrix was calcinated at different ranges of temperature from 200 to 600 C in order to obtain the c-OHAp powder. The results show the presence of c-OHAp a as unique phase. The thermal analysis indicates that the c-OHAp phase was obtained at 600 C. The particle size of the obtained material was\50 nm | - |
dc.publisher | Springer Nature | - |
dc.rights | closedAccess | - |
dc.subject | Polyesterification | - |
dc.subject | Hydroxyapatite | - |
dc.subject | Particle size | - |
dc.subject | Pechini method | - |
dc.title | Synthesis of nanosized carbonated apatite by a modified Pechini method: hydroxyapatite nucleation from a polymeric matrix | - |
dc.type | artículo | - |
dc.identifier.doi | 10.1007/s10971-014-3478-2 | - |
dc.date.updated | 2015-05-22T10:38:10Z | - |
dc.description.version | Peer Reviewed | - |
dc.language.rfc3066 | eng | - |
dc.type.coar | http://purl.org/coar/resource_type/c_6501 | es_ES |
item.fulltext | No Fulltext | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.openairetype | artículo | - |
item.cerifentitytype | Publications | - |
item.grantfulltext | none | - |
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